Carbon black tester

For determination of carbon black content in olefin materials like polye-thylene or polypropylene that do not contain non-volatile additives or fillers. Complying with the standards ASTM D 1603, ISO 18553 and ISO 6964. 

Product highlights

  • high accuracy
  • upgradeable
  • flexible build-up
  • reliable test results
  • intuitive operation

Description

The Purpose of Carbon Black test

The Carbon Black Test Equipment is engineered in accordance with ASTM D1603 and ISO 6964 standards, providing a reliable solution for determining carbon black content in thermoplastic materials such as polyethylene (PE), polypropylene (PP), and polybutene (PB). The analysis is performed using a high-precision gravimetric method, where the sample undergoes controlled pyrolysis in a nitrogen atmosphere. During this process, the polymer matrix decomposes, leaving behind carbon black and any inorganic residues.

The carbon black content is calculated by measuring the difference in sample weight before and after thermal treatment, ensuring accurate, repeatable, and standards-compliant results. This method is widely used in quality control, material verification, and plastics testing laboratories.

Important: This method is not suitable for materials containing non-volatile pigments or inorganic additives, as these substances may remain as residue and lead to inaccurate carbon black measurements

We offer two systems – for ASTM D1603-20 and ISO 6964-19. The two systems  both consists of complete setups for the test.

  • Tube furnace (electrical heated) for pyrolysis and oxydation of the sample material
  • Flow meter – according to the relevant standard
  • Glass – Combustion glass and glass for cleaning nitrogen (must be 99,998) and gas washing bottles (required unless laboratory is equipped with adequate exhaust ventilatio).
  • Combustion porcelain boats
  • Muffle oven heating the combustion boats to red heat to ensure no contamination of the test.

The Carbon black test procedure

Tests may be performed for the determination of the carbon black content of thermoplastic materials, such as: polyethylene, polypropylene and polybutene. The carbon black content is determined by means of weight difference.

The Carbon Black systems complies with tthe requirements of the ASTM D1603-20 and ISO 6964-19 standards 

    • Sample prep: Select representative polyethylene specimen. Cut to size, clean, and accurately weigh (record initial mass)
    • Pyrolysis (inert atmosphere): Place specimen in combustion tube.Purge with nitrogen (inert environment) Heat to ~600 °C → polymer decomposes (no burning). Residue left: carbon black + inorganic fillers.
    • Combustion (oxidation): Switch gas from nitrogen to oxygen. Maintain temperature to burn off carbon black. Remaining material = ash (inorganic fillers)
    • Weighing & analysis: Weigh residue after pyrolysis and final ash. Determine carbon black from mass loss during oxidation
    • Calculation & reporting: Carbon black % = mass loss (carbon black) vs. initial mass. Report: initial weight, pyrolysis residue, ash, % carbon black. Document conditions and retain data for traceability.

For more information and technical specifications please see the brochure.

Associated equipment to the carbon black tester

Associated equipment

Standards:

Specifications

Specimen size:

one to a few grams.

Tube furnace:

up 1200° Celsius

Muffle oven:

up 1100° Celsius
Inner dimension: W:160 x D140 x H100 mm, Volume 3 L.

Temperature control:

Programmable LCD display, more language possible

Dimensions:

Tube Furnace. W:434 x D340 x H508 mm excl. tube Weight 22 kg.
Muffle Oven: W:385 x D:330 x H: 405 + 155 (chimney) mm. Weight 21 kg.

Electrical supply:

120 V or 220-240 V, 50/60 Hz, single phased

Download ISO 6964-19 brochure

Download ASTM D1603-20 brochure

Associated products

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Standards

There are numerous international standards referring to testing. We supply testing equipment to fulfill any national and international testing standard within our field of business. In case you do not find the standard you are looking for in the below list, please contact us for further information

CASES

A story from the real world

Laboratory manager, WL Plastic
Occupation,

‘The SCITEQ lab saw is running great. It has cut our sample prep time in half’.

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